3-[(E)-2,4-Dichlorobenzylidene]-1-methylpiperidin-4-one
نویسندگان
چکیده
The piperidine ring of the title compound, C(13)H(13)Cl(2)NO, adopts an envelope conformation. Inter-molecular C-H⋯O inter-actions link the mol-ecules into a C(7) chain running along the b axis.
منابع مشابه
4-Chloro-N-[(E)-2,4-dichlorobenzylidene]aniline
In the mol-ecule of the title compound, C(13)H(8)Cl(3)N, the 4-chloro-aniline and 2,4-dichloro-benzaldehyde moieties are planar with r.m.s. deviation of 0.0115 and 0.0116 Å, respectively, and are oriented at a dihedral angle of 13.94 (8)°.
متن کامل1-(2,4-Dichlorobenzylidene)-4-ethylthiosemicarbazide
The title compound, C(10)H(11)Cl(2)N(3)S, was prepared by the reaction of 4-ethyl-thio-semicarbazide and 2,4-dichloro-benzaldehyde. It is approximately planar, the dihedral angle between the benzene ring and the thio-urea unit being 8.43 (18)°. In the crystal, inversion dimers linked by pairs of N-H⋯S hydrogen bonds generate R(2) (2)(8) loops.
متن کاملN′-(2,4-Dichlorobenzylidene)-3-methoxybenzohydrazide
There are two independent mol-ecules in the asymmetric unit of the title compound, C(15)H(12)Cl(2)N(2)O(2). The dihedral angle between the two benzene rings is 27.6 (4)° in one mol-ecule and 16.4 (4)° in the other. Both mol-ecules adopt an E configuration about the C=N bonds. In the crystal structure, mol-ecules are linked through inter-molecular N-H⋯O hydrogen bonds, forming chains in the a-ax...
متن کامل5′′-(2,4-Dichlorobenzylidene)-1′-(2,4-dichlorophenyl)-1′′-methyl-1′,2′,3′,5′,6′,7′,8′,8a’-octahydrodispiro[acenaphthylene-1,3′-indolizine-2′,3′′-piperidine]-2,4′′(1H)-dione
In the title compound, C(37)H(30)Cl(4)N(2)O(2), the pyridinone ring adopts a twisted half-chair conformation. In the octa-hydro-indolizine fused-ring system, the piperidine ring is in a chair conformation and the pyrrole ring is twisted about the C-N bond linking the five- and six-membered rings. The mol-ecular structure features an intra-molecular C-H⋯O inter-action and the crystal packing is ...
متن کامل3-(2,4-Dichlorobenzylidene)-1,5-dioxaspiro[5.5]undecane-2,4-dione
In the title mol-ecule, C(16)H(14)Cl(2)O(4), the 1,3-dioxane and cyclo-hexane rings exhibit distorted boat and chair conformations, respectively. In the crystal, a pair of weak inter-molecular C-H⋯O hydrogen bonds link the mol-ecules into an inversion dimer.
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عنوان ژورنال:
دوره 64 شماره
صفحات -
تاریخ انتشار 2008